Epoxy composites were prepared by doping nano Zirconia Toughened Alumina (ZTA) which were synthesized by solution combustion method into epoxy resin and hardener. Initially ZTA nanopowder was characterized to check its purity, morphology and to confirm its metal-oxide bonding using XRD, SEM and FTIR respectively. The thermal properties such as TGA and DTG were also analysed. The polymer composites were obtained by uniformly dispersing ZTA nanopowder into epoxy using an ultrasonicator. Polymer composites of various concentrations viz, 0.5, 1, 1.5, 2 and 2.5 wt% were synthesized, all concentrations were prepared on weight basis. All the polymer composites were tested for compression properties, flexural properties and tensile properties. Best results for all the mechanical properties were obtained for epoxy with 1.5 wt% ZTA composites. Electrical properties such as breakdown voltage and breakdown strength were analysed and outstanding results were observed for epoxy with 2.5 wt% ZTA composite.
Citation: Chaitra Srikanth, G.M. Madhu, Shreyas J. Kashyap. Enhanced structural, thermal, mechanical and electrical properties of nano ZTA/epoxy composites[J]. AIMS Materials Science, 2022, 9(2): 214-235. doi: 10.3934/matersci.2022013
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Epoxy composites were prepared by doping nano Zirconia Toughened Alumina (ZTA) which were synthesized by solution combustion method into epoxy resin and hardener. Initially ZTA nanopowder was characterized to check its purity, morphology and to confirm its metal-oxide bonding using XRD, SEM and FTIR respectively. The thermal properties such as TGA and DTG were also analysed. The polymer composites were obtained by uniformly dispersing ZTA nanopowder into epoxy using an ultrasonicator. Polymer composites of various concentrations viz, 0.5, 1, 1.5, 2 and 2.5 wt% were synthesized, all concentrations were prepared on weight basis. All the polymer composites were tested for compression properties, flexural properties and tensile properties. Best results for all the mechanical properties were obtained for epoxy with 1.5 wt% ZTA composites. Electrical properties such as breakdown voltage and breakdown strength were analysed and outstanding results were observed for epoxy with 2.5 wt% ZTA composite.
Let C be the complex plane. Denote by CN the N-dimensional complex Euclidean space with the inner product ⟨z,w⟩=∑Nj=1zj¯wj; by |z|2=⟨z,z⟩; by H(CN) the set of all holomorphic functions on CN; and by I the identity operator on CN.
The Fock space F2(CN) is a Hilbert space of all holomorphic functions f∈H(CN) with the inner product
⟨f,g⟩=1(2π)N∫CNf(z)¯g(z)e−12|z|2dν(z), |
where ν(z) denotes Lebesgue measure on CN. To simplify notation, we will often use F2 instead of F2(CN), and we will denote by ‖f‖ the corresponding norm of f. The reproducing kernel functions of the Fock space are given by
Kw(z)=e⟨z,w⟩2,z∈CN, |
which means that if f∈F2, then f(z)=⟨f,Kz⟩ for all z∈CN. It is easy to see that ‖Kw‖=e|w|2/4. Therefore, the following evaluation holds:
|f(z)|≤e|z|24‖f‖ |
for f∈F2 and z∈CN. If kw is the normalization of Kw, then
kw(z)=e⟨z,w⟩2−|w|24,z∈CN. |
Indeed, F2 is used to describe systems with varying numbers of particles in the states of quantum harmonic oscillators. On the other hand, the reproducing kernels in F2 are used to describe the coherent states in quantum physics. See [17] for more about the Fock space, and see [1,7,11] for the studies of some operators on the Fock space.
For a given holomorphic mapping φ:CN→CN and u∈H(CN), the weighted composition operator, usually denoted by Wu,φ, on or between some subspaces of H(CN) is defined by
Wu,φf(z)=u(z)f(φ(z)). |
When u=1, it is the composition operator, usually denoted by Cφ. While φ(z)=z, it is the multiplication operator, usually denoted by Mu.
Forelli in [8] proved that the isometries on Hardy space Hp defined on the open unit disk (for p≠2) are certain weighted composition operators, which can be regarded as the earliest presence of the weighted composition operators. Weighted composition operators have also been used in descriptions of adjoints of composition operators (see [4]). An elementary problem is to provide function-theoretic characterizations for which the symbols u and φ induce a bounded or compact weighted composition operator on various holomorphic function spaces. There have been many studies of the weighted composition operators and composition operators on holomorphic function spaces. For instance, several authors have recently worked on the composition operators and weighted composition operators on Fock space. For the one-variable case, Ueki [13] characterized the boundedness and compactness of weighted composition operators on Fock space. As a further work of [13], Le [10] found the easier criteria for the boundedness and compactness of weighted composition operators. Recently, Bhuia in [2] characterized a class of C-normal weighted composition operators on Fock space.
For the several-variable case, Carswell et al. [3] studied the boundedness and compactness of composition operators. From [3], we see that the one-variable case composition operator Cφ is bounded on Fock space if and only if φ(z)=az+b, where |a|≤1, and if |a|=1, then b=0. Let A:CN→CN be a linear operator. Zhao [14,15,16] characterized the unitary, invertible, and normal weighted composition operator Wu,φ on Fock space, when φ(z)=Az+b and u=kc. Interestingly enough, Zhao [15] proved that for φ(z)=Az+b and u(z)=Kc(z), weighted composition operator Wu,φ is bounded on Fock space if and only if ‖A‖≤1 and ⟨Aζ,b+Ac⟩=0 whenever |Aζ|=|ζ| for ζ∈CN.
Motivated by the above-mentioned interesting works, for the special symbols φ(z)=Az+b and u=Kc, here we study the adjoint, self-adjointness, and hyponormality of weighted composition operators on Fock space. Such properties of the abstract or concrete operators (for example, Toeplitz operators, Hankel operators, and composition operators) have been extensively studied on some other holomorphic function spaces. This paper can be regarded as a continuation of the weighted composition operators on Fock space.
In this section, we characterize the adjoints of weighted composition operators Wu,φ on Fock space, where φ(z)=Az+b and u=Kc.
We first have the following result:
Lemma 2.1. Let A, B:CN→CN be linear operators with ‖A‖≤1 and ‖B‖≤1, φ(z)=Az+a, ψ(z)=Bz+b for a,b∈CN, and the operators Cφ and Cψ be bounded on F2. Then
C∗φCψ=WKa,BA∗z+b, |
where A∗ is the adjoint operator of A.
Proof. From Lemma 2 in [3], it follows that
C∗φCψ=MKaCA∗zCBz+b=MKaC(Bz+b)∘A∗z=MKaCBA∗z+b=WKa,BA∗z+b, |
from which the result follows. The proof is complete.
In Lemma 2.1, we prove that the product of the adjoint of a composition operator and another composition operator is expressed as a weighted composition operator. Next, we will see that in some sense, the converse of Lemma 2.1 is also true. Namely, we will prove that if φ(z)=Az+b, where A:CN→CN is a linear operator with ‖A‖<1, and u=Kc, then the operator Wu,φ on F2 can be written as the product of the adjoint of a composition operator and another composition operator.
Lemma 2.2. Let A:CN→CN be a linear operator with ‖A‖<1. If A and c satisfy the condition ⟨A∗ζ,c⟩=0 whenever |A∗ζ|=|ζ|, then there exists a positive integer n such that the operator Wu,φ on F2 defined by φ(z)=Az+b and u(z)=Kc(z) is expressed as
Wu,φ=C∗n+1nA∗z+cCnn+1z+b. |
Proof. From Theorem 2 in [3], we see that the operator CA∗z+c is bounded on F2. Since ‖A∗‖<1, there exists a large enough positive integer n such that
‖(1+1n)A∗‖≤1. |
Also, by Theorem 2 in [3], the operator Cn+1nA∗z+c is bounded on F2, which implies that the operator C∗n+1nA∗z+c is also bounded on F2. Since |nn+1Iζ|=|ζ| if and only if ζ=0, ⟨nn+1Iζ,b⟩=0 whenever |nn+1Iζ|=|ζ|. By Theorem 2 in [3], the operator Cnn+1Iz+b is bounded on F2. Then, it follows from Lemma 2.1 that
C∗n+1nA∗z+cCnn+1Iz+b=WKc,Az+b. |
The proof is complete.
Now, we can obtain the adjoint for some weighted composition operators.
Theorem 2.1. Let φ(z)=Az+b, u(z)=Kc(z), and A and c satisfy ⟨A∗ζ,c⟩=0 whenever |A∗ζ|=|ζ|. Then it holds that
W∗u,φ=WKb,A∗z+c. |
Proof. In Lemma 2.2, we have
Wu,φ=C∗n+1nA∗z+cCnn+1Iz+b. | (2.1) |
It follows from (2.1) that
W∗u,φ=C∗nn+1Iz+bCn+1nA∗z+c. | (2.2) |
Therefore, from (2.2) and Lemma 2.1, the desired result follows. The proof is complete.
By using the kernel functions, we can obtain the following result:
Lemma 2.3. Let the operator Wu,φ be a bounded operator on F2. Then it holds that
W∗u,φKw=¯u(w)Kφ(w). |
Proof. Let f be an arbitrary function in F2. We see that
⟨W∗u,φKw,f⟩=⟨Kw,Wu,φf⟩=¯⟨Wu,φf,Kw⟩=¯u(w)f(φ(w))=¯u(w)⟨Kφ(w),f⟩. |
From this, we deduce that W∗u,φKw=¯u(w)Kφ(w). The proof is complete.
Here, we characterize the self-adjoint weighted composition operators.
Theorem 2.2. Let A:CN→CN be a linear operator, b,c∈CN, φ(z)=Az+b, u(z)=Kc(z), and the operator Wu,φ be bounded on F2. Then the operator Wu,φ is self-adjoint on F2 if and only if A:CN→CN is self-adjoint and b=c.
Proof. In Lemma 2.3, we have
W∗u,φKw(z)=¯u(w)Kφ(w)=¯Kc(w)e⟨z,φ(w)⟩2=e⟨c,w⟩2e⟨z,Aw+b⟩2. | (2.3) |
On the other hand,
Wu,φKw(z)=u(z)Kw(φ(z))=e⟨z,c⟩2e⟨Az+b,w⟩2. | (2.4) |
It is clear that operator Wu,φ is self-adjoint on F2 if and only if
W∗u,φKw=Wu,φKw. |
From (2.3) and (2.4), it follows that
e⟨c,w⟩2e⟨z,Aw+b⟩2=e⟨z,c⟩2e⟨Az+b,w⟩2. | (2.5) |
Letting z=0 in (2.5), we obtain that e⟨c,w⟩2=e⟨b,w⟩2 which implies that
⟨c,w⟩−⟨b,w⟩=4kπi, | (2.6) |
where k∈N. Also, letting w=0 in (2.6), we see that k=0. This shows that ⟨c,w⟩−⟨b,w⟩=0, that is, ⟨c,w⟩=⟨b,w⟩. From this, we deduce that b=c. Therefore, (2.5) becomes e⟨z,Aw⟩2=e⟨Az,w⟩2. From this, we obtain that ⟨z,Aw⟩=⟨Az,w⟩, which implies that ⟨A∗z,w⟩=⟨Az,w⟩. This shows that A=A∗, that is, A:CN→CN is self-adjoint.
Now, assume that A is a self-adjoint operator on CN and b=c. A direct calculation shows that (2.5) holds. Then Wu,φ is a self-adjoint operator on F2. The proof is complete.
In [14], Zhao proved that the operator Wu,φ on F2 is unitary if and only if there exist an unitary operator A:CN→CN, a vector b∈CN, and a constant α with |α|=1 such that φ(z)=Az−b and u(z)=αKA−1b(z). Without loss of generality, here we characterize the self-adjoint unitary operator Wu,φ on F2 for the case α=1 and obtain the following result from Theorem 2.2.
Corollary 2.1. Let A:CN→CN be a unitary operator and b∈CN such that φ(z)=Az−b and u(z)=KA−1b(z). Then the operator Wu,φ is self-adjoint on F2 if and only if A:CN→CN is self-adjoint and Ab+b=0.
First, we recall the definition of hyponormal operators. An operator T on a Hilbert space H is said to be hyponormal if ‖Ax‖≥‖A∗x‖ for all vectors x∈H. T is called co-hyponormal if T∗ is hyponormal. In 1950, Halmos, in his attempt to solve the invariant subspace problem, extended the notion of normal operators to two new classes, one of which is now known as the hyponormal operator (see [9]). Clearly, every normal operator is hyponormal. From the proof in [6], it follows that T is hyponormal if and only if there exists a linear operator C with ‖C‖≤1 such that T∗=CT. In some sense, this result can help people realize the characterizations of the hyponormality of some operators. For example, Sadraoui in [12] used this result to characterize the hyponormality of composition operators defined by the linear fractional symbols on Hardy space. On the other hand, some scholars studied the hyponormality of composition operators on Hardy space by using the fact that the operator Cφ on Hardy space is hyponormal if and only if
‖Cφf‖2≥‖C∗φf‖2 |
for all f in Hardy space. For example, Dennis in [5] used the fact to study the hyponormality of composition operators on Hardy space. In particular, this inequality for norms is used when f is a reproducing kernel function Kw for any w∈CN. Actually, to the best of our knowledge, there are few studies on the hyponormality of weighted composition operators. Here, we consider this property of weighted composition operators on Fock space.
First, we have the following result, which can be proved by using the reproducing kernel functions.
Lemma 3.1. Let w∈CN and the operator Wu,φ be bounded on F2. Then
‖Wu,φKw‖2=W∗u,φWu,φKw(w). |
Proof. From the inner product, we have
‖Wu,φKw‖2=⟨Wu,φKw,Wu,φKw⟩=⟨W∗u,φWu,φKw,Kw⟩=W∗u,φWu,φKw(w). |
The proof is complete.
Theorem 3.1. Let A:CN→CN be a linear operator, φ(z)=Az+b, u=kc, and the operator Wu,φ be bounded on F2. If the operator Wu,φ is hyponormal on F2, then A∗b−b=Ac−c and |b|≤|c|.
Proof. From a direct calculation, we have
Wu,φKw(z)=u(z)Kw(φ(z))=kc(z)Kw(Az+b)=e⟨z,c⟩2−|c|24e⟨Az+b,w⟩2=e⟨z,A∗w+c⟩+⟨b,w⟩2−|c|24=e⟨b,w⟩2−|c|24KA∗w+c(z). | (3.1) |
From (3.1), it follows that
W∗u,φWu,φKw(z)=e⟨b,w⟩2−|c|24W∗u,φKA∗w+c(z)=e⟨b,w⟩2−|c|24¯u(A∗w+c)Kφ(A∗w+c)(z)=e⟨b,w⟩2+⟨c,A∗w+c⟩2+⟨z,AA∗w+Ac+b⟩2−|c|22=e⟨b+Ac,w⟩2+⟨z,AA∗w⟩2+⟨z,Ac+b⟩2. | (3.2) |
On the other hand, we also have
Wu,φW∗u,φKw(z)=¯u(w)Wu,φKφ(w)(z)=¯u(w)u(z)Kφ(w)(φ(z))=e⟨c,w⟩2+⟨z,c⟩2+⟨Az+b,Aw+b⟩2−|c|22=e⟨c+A∗b,w⟩2+|b|22+⟨z,AA∗w⟩2+⟨z,c+A∗b⟩2−|c|22. | (3.3) |
From Lemma 3.1, (3.2), and (3.3), it follows that
‖W∗u,φKw‖2=Wu,φW∗u,φKw(w)=e⟨c+A∗b,w⟩2+|b|22+|A∗w|22+⟨w,c+A∗b⟩2−|c|22 |
and
‖Wu,φKw‖2=W∗u,φWu,φKw(w)=e⟨b+Ac,w⟩2+|A∗w|22+⟨w,Ac+b⟩2. |
Then, we have
‖W∗u,φKw‖2−‖Wu,φKw‖2=e|A∗w|22(e⟨c+A∗b,w⟩2+|b|22+⟨w,c+A∗b⟩2−|c|22−e⟨b+Ac,w⟩2+⟨w,Ac+b⟩2), |
which shows that
‖W∗u,φKw‖2−‖Wu,φKw‖2≤0 |
for all w∈CN if and only if
e⟨c+A∗b,w⟩2+|b|22+⟨w,c+A∗b⟩2−|c|22≤e⟨b+Ac,w⟩2+⟨w,Ac+b⟩2. | (3.4) |
It is clear that (3.4) holds if and only if
⟨c+A∗b,w⟩+|b|2+⟨w,c+A∗b⟩−|c|2≤⟨b+Ac,w⟩+⟨w,Ac+b⟩. | (3.5) |
From (3.5), we see that (3.4) holds if and only if
⟨A∗b−Ac+c−b,w⟩+⟨w,A∗b−Ac+c−b⟩+|b|2−|c|2≤0. | (3.6) |
Therefore, we deduce that (3.4) holds for all w∈CN if and only if |b|≤|c| and A∗b−b=Ac−c. The proof is complete.
If b=c=0 in Theorem 3.1, then Wu,φ is reduced into the composition operator CAz. For this case, Theorem 3.1 does not provide any useful information on the operator A:CN→CN when CAz is hyponormal on F2. However, we have the following result, which completely characterizes the hyponormal composition operators:
Theorem 3.2. Let A:CN→CN be a linear operator such that CAz is bounded on F2. Then the operator CAz is hyponormal on F2 if and only if A:CN→CN is co-hyponormal.
Proof. Assume that A:CN→CN is co-hyponormal. Then there exists an operator B:CN→CN with ‖B‖≤1 such that A=BA∗. We therefore have
C∗Az=CA∗z=CAB∗z=CB∗zCAz. |
Next, we want to show that ‖CB∗z‖=1. By Theorem 4 in [3], we have
‖CB∗z‖=e14(|w0|2−|B∗w0|2), | (3.7) |
where w0 is any solution to (I−BB∗)w=0. From this, we obtain that w0=BB∗w0, and then
|B∗w0|2=⟨B∗w0,B∗w0⟩=⟨w0,BB∗w0⟩=⟨w0,w0⟩=|w0|2. | (3.8) |
Thus, by considering (3.7) and (3.8), we see that ‖CB∗z‖=1. It follows that the operator CAz is hyponormal on F2.
Now, assume that the operator CAz is hyponormal on F2. Then there exists a linear operator C on F2 with ‖C‖≤1 such that C∗Az=CCAz. By Lemma 2 in [3], we have C∗Az=CA∗z. This shows that CCAz is a composition operator. This result shows that there exists a holomorphic mapping φ:CN→CN such that C=Cφ. So A∗z=A(φ(z)) for all z∈CN, which implies that there exists a linear operator B:CN→CN such that φ(z)=B∗z, and then C=CB∗z. Therefore, A∗=AB∗, that is, A=BA∗. Since ‖C‖≤1, this shows that the operator C=CB∗z is bounded on F2. From Lemma 2.3 in [15], we obtain that ‖B∗‖≤1, which also shows that ‖B‖≤1 since ‖B∗‖=‖B‖. We prove that A:CN→CN is co-hyponormal. The proof is complete.
Remark 3.1. In the paper, we only obtain a necessary condition for the hyponormality of weighted composition operators on Fock space. We hope that the readers can continuously consider the problem in Fock space.
In this paper, I give a proper description of the adjoint W∗u,φ on Fock space for the special symbol functions u(z)=Kc(z) and φ(z)=Az+b. However, it is difficult to give a proper description of the general symbols. On the other hand, I consider the hyponormal weighted composition operators on Fock space and completely characterize hyponormal composition operators on this space. I hope that people are interested in the research in this paper.
The authors declare they have not used Artificial Intelligence (AI) tools in the creation of this article.
This study was supported by Sichuan Science and Technology Program (2024NSFSC0416).
The author declares that he has no competing interests.
[1] |
Wetzel B, Haupert F, Zhang MQ (2003) Epoxy nanocomposites with high mechanical and tribological performance. Compos Sci Technol 63: 2055-2067. https://doi.org/10.1016/S0266-3538(03)00115-5 doi: 10.1016/S0266-3538(03)00115-5
![]() |
[2] |
Carolan D, Ivankovic A, Kinloch AJ, et al. (2017) Toughened carbon fibre-reinforced polymer composites with nanoparticle-modified epoxy matrices. J Mater Sci 52: 1767-1788. https://doi.org/10.1007/s10853-016-0468-5 doi: 10.1007/s10853-016-0468-5
![]() |
[3] |
Dorigato A, Pegoretti A, Bondioli F, et al. (2010) Improving epoxy adhesives with zirconia nanoparticles. Compos Interface 17: 873-892. https://doi.org/10.1163/092764410X539253 doi: 10.1163/092764410X539253
![]() |
[4] |
Bondioli F, Cannillo V, Fabbri E, et al. (2006) Preparation and characterization of epoxy resins filled with submicron spherical zirconia particles. Polimery 51: 794-798. https://doi.org/10.14314/polimery.2006.794 doi: 10.14314/polimery.2006.794
![]() |
[5] |
Dorigato A, Pegoretti A (2011) The role of alumina nanoparticles in epoxy adhesives. J Nanopart Res 13: 2429-2441. https://doi.org/10.1007/s11051-010-0130-0 doi: 10.1007/s11051-010-0130-0
![]() |
[6] |
Yu ZQ, You SL, Yang ZG, et al. (2011) Effect of surface functional modification of nano-alumina particles on thermal and mechanical properties of epoxy nanocomposites. Adv Compos Mater 20: 487-502. https://doi.org/10.1163/092430411X579104 doi: 10.1163/092430411X579104
![]() |
[7] |
Reyes-Rojas A, Dominguez-Rios C, Garcia-Reyes A, et al. (2018) Sintering of carbon nanotube-reinforced zirconia-toughened alumina composites prepared by uniaxial pressing and cold isostatic pressing. Mater Res Express 5: 105602. https://doi.org/10.1088/2053-1591/aada35 doi: 10.1088/2053-1591/aada35
![]() |
[8] | Chuankrerkkul N, Somton K, Wonglom T, et al. (2016) Physical and mechanical properties of zirconia toughened alumina (ZTA) composites fabricated by powder injection moulding. Chiang Mai J Sci 43: 375-380. |
[9] |
Ponnilavan V, Kannan S (2019) Structural, optical tuning, and mechanical behavior of zirconia toughened alumina through europium substitutions. J Biomed Mater Res Part B 107: 1170-1179. https://doi.org/10.1002/jbm.b.34210 doi: 10.1002/jbm.b.34210
![]() |
[10] |
Srikanth C, Madhu GM (2020) Effect of ZTA concentration on structural, thermal, mechanical and dielectric behavior of novel ZTA-PVA nanocomposite films. SN Appl Sci 2: 1-12. https://doi.org/10.1007/s42452-020-2232-3 doi: 10.1007/s42452-020-2232-3
![]() |
[11] |
Zhang J, Ge L, Chen ZG, et al. (2019) Cracking behavior and mechanism of gibbsite crystallites during calcination. Cryst Res Technol 54: 1800201. https://doi.org/10.1002/crat.201800201 doi: 10.1002/crat.201800201
![]() |
[12] |
Bhaduri S, Bhaduri SB, Zhou E (1998) Auto ignition synthesis and consolidation of Al2O3-ZrO2 nano/nano composite powders. J Mater Res 13: 156-165. https://doi.org/10.1557/JMR.1998.0021 doi: 10.1557/JMR.1998.0021
![]() |
[13] |
Vasylkiv O, Sakka Y, Skorokhod VV (2003) Low-temperature processing and mechanical properties of zirconia and zirconia-alumina nanoceramics. J Am Ceram Soc 86: 299-304. https://doi.org/10.1111/j.1151-2916.2003.tb00015.x doi: 10.1111/j.1151-2916.2003.tb00015.x
![]() |
[14] |
Sagar JS, Kashyap SJ, Madhu GM, et al. (2020) Investigation of mechanical, thermal and electrical parameters of gel combustion-derived cubic zirconia/epoxy resin composites for high-voltage insulation. Cerâmica 66: 186-196. https://doi.org/10.1590/0366-69132020663782887 doi: 10.1590/0366-69132020663782887
![]() |
[15] |
Ho MW, Lam CK, Lau K, et al. (2006) Mechanical properties of epoxy-based composites using nanoclays. Compos Struct 75: 415-421. https://doi.org/10.1016/j.compstruct.2006.04.051 doi: 10.1016/j.compstruct.2006.04.051
![]() |
[16] |
Uhl FM, Davuluri SP, Wong SC, et al. (2004) Organically modified montmorillonites in UV curable urethane acrylate films. Polymer 45: 6175-6187. https://doi.org/10.1016/j.polymer.2004.07.001 doi: 10.1016/j.polymer.2004.07.001
![]() |
[17] |
Nguyen TA, Nguyen TV, Thai H, et al. (2016) Effect of nanoparticles on the thermal and mechanical properties of epoxy coatings. J Nanosci Nanotechnol 16: 9874-9881. https://doi.org/10.1166/jnn.2016.12162 doi: 10.1166/jnn.2016.12162
![]() |
[18] |
Baiquni M, Soegijono B, Hakim AN (2019) Thermal and mechanical properties of hybrid organoclay/rockwool fiber reinforced epoxy composites. J Phys Conf Ser 1191: 012056. https://doi.org/10.1088/1742-6596/1191/1/012056 doi: 10.1088/1742-6596/1191/1/012056
![]() |
[19] |
Zhang X, Alloul O, He Q, et al. (2013) Strengthened magnetic epoxy nanocomposites with protruding nanoparticles on the graphene nanosheets. Polymer 54: 3594-3604. https://doi.org/10.1016/j.polymer.2013.04.062 doi: 10.1016/j.polymer.2013.04.062
![]() |
[20] |
Nazarenko OB, Melnikova TV, Visakh PM (2016) Thermal and mechanical characteristics of polymer composites based on epoxy resin, aluminium nanopowders and boric acid. J Phys Conf Ser 671: 012040. https://doi.org/10.1088/1742-6596/671/1/012040 doi: 10.1088/1742-6596/671/1/012040
![]() |
[21] |
Sand Chee S, Jawaid M (2019) The effect of Bi-functionalized MMT on morphology, thermal stability, dynamic mechanical, and tensile properties of epoxy/organoclay nanocomposites. Polymers 11: 2012. https://doi.org/10.3390/polym11122012 doi: 10.3390/polym11122012
![]() |
[22] |
Bikiaris D (2011) Can nanoparticles really enhance thermal stability of polymers? Part Ⅱ: An overview on thermal decomposition of polycondensation polymers. Thermochim Acta 523: 25-45. https://doi.org/10.1016/j.tca.2011.06.012 doi: 10.1016/j.tca.2011.06.012
![]() |
[23] |
Xue Y, Shen M, Zeng S, et al. (2019) A novel strategy for enhancing the flame resistance, dynamic mechanical and the thermal degradation properties of epoxy nanocomposites. Mater Res Express 6: 125003. https://doi.org/10.1088/2053-1591/ab537f doi: 10.1088/2053-1591/ab537f
![]() |
[24] |
Colomban P (1989) Structure of oxide gels and glasses by infrared and Raman scattering. J Mater Sci 24: 3011-3020. https://doi.org/10.1007/BF02385660 doi: 10.1007/BF02385660
![]() |
[25] |
Taavoni-Gilan A, Taheri-Nassaj E, Naghizadeh R, et al. (2010) Properties of sol-gel derived Al2O3-15 wt% ZrO2 (3 mol% Y2O3) nanopowders using two different precursors. Ceram Int 36: 1147-1153. https://doi.org/10.1016/j.ceramint.2009.11.011 doi: 10.1016/j.ceramint.2009.11.011
![]() |
[26] |
Noma T, Sawaoka A (1984) Fracture toughness of high pressure sintered Al2O3-ZrO2 ceramics. J Mater Sci Lett 3: 533-535. https://doi.org/10.1007/BF00720992 doi: 10.1007/BF00720992
![]() |
[27] |
Shukla DK, Kasisomayajula SV, Parameswaran V (2008) Epoxy composites using functionalized alumina platelets as reinforcements. Compos Sci Technol 68: 3055-3063. https://doi.org/10.1016/j.compscitech.2008.06.025 doi: 10.1016/j.compscitech.2008.06.025
![]() |
[28] |
Abbate M, Martuscelli E, Musto P, et al. (1994) Toughening of a highly cross-linked epoxy resin by reactive blending with bisphenol A polycarbonate. I. FTIR spectroscopy. J Polym Sci Pol Phys 32: 395-408. https://doi.org/10.1002/polb.1994.090320301 doi: 10.1002/polb.1994.090320301
![]() |
[29] |
Katon JE, Bentley FF (1963) New spectra-structure correlations of ketones in the 700-750 cm-1 region. Spectrochim Acta 19: 639-653. https://doi.org/10.1016/0371-1951(63)80127-7 doi: 10.1016/0371-1951(63)80127-7
![]() |
[30] |
Magnani G, Brillante A (2005) Effect of the composition and sintering process on mechanical properties and residual stresses in zirconia-alumina composites. J Eur Ceram Soc 25: 3383-3392. https://doi.org/10.1016/j.jeurceramsoc.2004.09.025 doi: 10.1016/j.jeurceramsoc.2004.09.025
![]() |
[31] |
Ashamol A, Priyambika VS, Avadhani GS, et al. (2013) Nanocomposites of crosslinked starch phthalate and silane modified nanoclay: Study of mechanical, thermal, morphological, and biodegradable characteristics. Starch-Stärke 65: 443-452. https://doi.org/10.1002/star.201200145 doi: 10.1002/star.201200145
![]() |
[32] |
Jumahat A, Soutis C, Mahmud J, et al. (2012) Compressive properties of nanoclay/epoxy nanocomposites. Procedia Eng 41: 1607-1613. https://doi.org/10.1016/j.proeng.2012.07.361 doi: 10.1016/j.proeng.2012.07.361
![]() |
[33] |
Abbass A, Abid S, Özakça M (2019) Experimental investigation on the effect of steel fibers on the flexural behavior and ductility of high-strength concrete hollow beams. Adv Civ Eng 2019: 8390345. https://doi.org/10.1155/2019/8390345 doi: 10.1155/2019/8390345
![]() |
[34] |
Konnola R, Deeraj BDS, Sampath S, et al. (2019) Fabrication and characterization of toughened nanocomposites based on TiO2 nanowire-epoxy system. Polym Compos 40: 2629-2638. https://doi.org/10.1002/pc.25058 doi: 10.1002/pc.25058
![]() |
[35] |
Zhao S, Schadler LS, Duncan R, et al. (2008) Mechanisms leading to improved mechanical performance in nanoscale alumina filled epoxy. Compos Sci Technol 68: 2965-2975. https://doi.org/10.1016/j.compscitech.2008.01.009 doi: 10.1016/j.compscitech.2008.01.009
![]() |
[36] |
Goyat MS, Rana S, Halder S, et al. (2018) Facile fabrication of epoxy-TiO2 nanocomposites: a critical analysis of TiO2 impact on mechanical properties and toughening mechanisms. Ultrason Sonochem 40: 861-873. https://doi.org/10.1016/j.ultsonch.2017.07.040 doi: 10.1016/j.ultsonch.2017.07.040
![]() |
[37] |
Johnsen BB, Kinloch AJ, Mohammed RD, et al. (2007) Toughening mechanisms of nanoparticle-modified epoxy polymers. Polymer 48: 530-541. https://doi.org/10.1016/j.polymer.2006.11.038 doi: 10.1016/j.polymer.2006.11.038
![]() |
[38] |
Johnsen BB, Kinloch AJ, Taylor AC (2005) Toughness of syndiotactic polystyrene/epoxy polymer blends: microstructure and toughening mechanisms. Polymer 46: 7352-7369. https://doi.org/10.1016/j.polymer.2005.05.151 doi: 10.1016/j.polymer.2005.05.151
![]() |
[39] |
Mohanty A, Srivastava VK (2013) Dielectric breakdown performance of alumina/epoxy resin nanocomposites under high voltage application. Mater Design 47: 711-716. https://doi.org/10.1016/j.matdes.2012.12.052 doi: 10.1016/j.matdes.2012.12.052
![]() |
![]() |
![]() |